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Bulletin of Chinese Academy of Sciences (Chinese Version)

Keywords

high-resolution mass spectrometry; pesticide residus data; intelligent analyzing; automatic generation of detection report

Document Type

Article

Abstract

A technical plaform for pesticide residues detection has been developed on the basis of tri-element integrated technology of highresolution MS-internet-digital science (simply referred as "tri-element integrated technology") inlcuding network leagued laboratories, detection result databases, and 4 sub-bases of fundamental data, data collection system as well as data intelligently analyzing system. The network leagued laboratoies located at various places across the country submit the raw test results of pesticide residues from their client side to the collection system per a unified template; the collection system shall obtain the data, supplement the information, consolidate the derivatives and analyze the toxicity before archiving and storing the results into the test result database based on the judgment of the contamination levels in referrence to maximum residule limit (MRL) of multi-countries. Data intelligent analyzing system shall, based on the settings of conditions by a client, access data, conduct various statistical analysis per the statisitical analytical module, churn out graphs/tables, derive a general conclusion and then return the analytical results to the client side of the network leagued laboratories. Hence the realization of "one-click download" of the detection report with graphs within 30 minutes, with its working efficiency being incomparable to that of the conventional method. The platform for pesticide residue detection data has realized the realtime detection of pesticide residues in edible agricultural products and timely collection, management and intelligent analysis of the data, which may give an automatic generation of the test report of the related pesticide residues within a short time, thus providing a realtime online service for the traceability and safety risk assessment of pesticide residues and the scientific management and application of pesticides. This is an effective and rapid tool for realizing the scientific application of pesticides, supervising the pesticide residue safety, and executing the "the safety of every bite" of our common folks.

First page

1384

Last Page

1396

Language

Chinese

Publisher

Bulletin of Chinese Academy of Sciences

References

杨杰, 樊永祥, 杨大进, 等.国际食品污染物监测体系理化指标监测介绍及思考.中国食品卫生杂志, 2009, 21(2):161-168.

许彦阳, 钱永忠.中美农产品药物残留监测计划比较分析及启示.世界农业, 2015, (7):5-9.

汤晓艳, 郭林宇, 王敏, 等.欧盟农药残留监控体系概况及启示.农业质量标准, 2009, (6):41-44.

The Japanese Positive List System for Agricultural Chemical Residues in Foods.[2006-05-29]. http://www.ffcr.or.jp/zaidan/FFCRHOME.nsf/pages/MRLs-p.

农业部. 关于发布《中华人民共和国动物及动物源食品中残留物质监控计划》和《官方取样程序》的通知(农牧发8号). [2003-07-04]. http://www.moa.gov.cn/zwllm/zcfg/qtbmgz/200601/t20060123_541427.htm.

中华人民共和国工业和信息化部. 关于印发《食品安全风险监测管理规定(试行)》的通知(卫监督发17号). [2010-01-25]. http://www.miit.gov.cn/n1146285/n1146352/n3054355/n3057601/n3057609/c3561870/content.html.

国家卫生计生委食品安全标准与监测评估司. GB 2763-2016食品安全国家标准食品中农药最大残留限量.北京:中国标准出版社, 2016.

庞国芳, 范春林, 常巧英等.追踪近20年SCI论文见证世界农药残留检测技术进步.食品科学, 2012, 33(Z1):1-7.

Pang G F, Fan C L, Cao Y Z, et al. High throughput analytical techniques for the determination and confirmation of residues of 653 multiclass pesticides and chemical pollutants in tea by GC/MS, GC/MS/MS, and LC/MS/MS:collaborative study, first action 2014.09. Journal of AOAC International, 2015, 98(5):1428-1454.

Núñez O, Gallart-Ayala H, Ferrer I, et al. Strategies for the multiresidue analysis of 100 pesticides by liquid chromatography-triple quadrupole mass spectrometry. Journal of Chromatography A, 2012, 1249(15):164-180.

He Z Y, Lu W, Yi P, et al. Multiresidue analysis of over 200 pesticides in cereals using a QuEChERS and gas chromatographytandem mass spectrometry-based method. Food Chemistry, 2015, 169:372-380.

Pizzutti I R, de Kok A, Hiematra M, et al. Method validation and comparison of acetonitrile and acetone extraction for the analysis of 169 pesticides in soya grain by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2009, 1216(21):4539-4552.

Walorczyk S, Drożdżyński D, Gnusowski B. Multiresidue determination of 160 pesticides in wines employing mixed-mode dispersive-solid phase extraction and gas chromatography-tandem mass spectrometry. Talanta, 2011, 85(4):1856-1870.

Kmellar B, Fodor P, Pareja L, et al. Validation and uncertainty study of a comprehensive list of 160 pesticide residues in multi-class vegetables by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2008, 1215(1-2):37-50.

Zhao M A, Feng Y N, Zhu Y Z, et al. Multi-residue method for determination of 238 pesticides in Chinese cabbage and Cucumber by liquid chromatography-tandem mass spectrometry:comparison of different purification procedures. Journal of Agricultural and Food Chemistry, 2014. 62(47):11449-11456.

Jadhav M R, Oulkar D P, Ahammed S T P, et al. Quantitative screening of agrochemical residues in fruits and vegetables by buffered ethyl acetate extraction and LC-MS/MS analysis. Journal of Agricultural and Food Chemistry, 2015, 63(18):4449-4456.

Botitsi H V, Garbis S D, Economou A, et al. Current mass spectrometry strategies for the analysis of pesticides and their metabolites in food and water matrices. Mass Spectrometry Reviews, 2011, 30(5):907-939.

Alder L, Steinborn A, Bergelt S, et al. Suitability of an orbitrap mass spectrometer for the screening of pesticide residues in extracts of fruits and vegetables. Journal of Aoac International, 2011, 94(6):1661-1673.

Gómez-Ramos M M, Ferrer C, Malato O, et al. Liquid chromatography-high-resolution mass spectrometry for pesticide residue analysis in fruit and vegetables:screening and quantitative studies. Journal of Chromatography A, 2013, 1287(8):24-37.

Wang Z, Cao Y, Ge N, et al., Wide-scope screening of pesticides in fruits and vegetables using information-dependent acquisition employing UHPLC-QTOF-MS and automated MS/MS library searching. Analytical and Bioanalytical Chemistry, 2016. 408(27):7795-7810.

冯超, 徐骞, 金玉娥, 等.植物源性食品中农药残留筛选平台研究.食品安全质量检测学报, 2015, 6(5):1646-1653.

杨永坛, 陈士恒, 史晓梅.食品中农药残留筛查系统的构建.食品安全质量检测学报, 2015, 6(4):1101-1106.

European Food Safety Authority. The 2011 European Union report on pesticide residues in food.[2014-07-23]. https://publications.europa.eu/en/publication-detail/-/publication/c9c0a018-9c6f-423b-b7db-c891103a4849/language-en.

国家质量监督检验检疫总局食品安全局, 中国检验检疫科学研究院.日本厚生劳动省食品中农用化学品残留检测方法.北京:中国标准出版社, 2006.

庞国芳, 常巧英, 范春林.农药残留监测技术研究与监控体系构建展望.中国科学院院刊, 2017, 32(10):1083-1090.

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